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Mixed sugar-nylon 14-, 28- and 42-membered ring macrocyclic lactams

Abstract:
Hydrogenation of linear ω-azido-pentafluorophenyl esters from mixed oligomers of 6-amino-6-deoxy-D-galactonic acid (or 6-amino-6-deoxy-D-mannonic acid) and 6-aminohexanoic acid gives cyclic peptides containing 14-, 28- and 42-membered ring lactams. Hydrogenation of a tetrameric peptide derived from ε-amino acids gave a 28-membered ring lactam in 79% yield. © 2003 Elsevier Ltd. All rights reserved.
Publication status:
Published

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
Journal:
TETRAHEDRON LETTERS
Volume:
45
Issue:
1
Pages:
163-166
Publication date:
2004-01-01
DOI:
ISSN:
0040-4039
URN:
uuid:c7ce130b-b4d9-421e-9d7e-34955626320f
Source identifiers:
38950
Local pid:
pubs:38950

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